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Simple and low-cost tabletop NMR system for chemical-shift-resolution spectra measurements.

Authors :
Hibino, Y.
Sugahara, K.
Muro, Y.
Tanaka, H.
Sato, T.
Kondo, Y.
Source :
Journal of Magnetic Resonance. Sep2018, Vol. 294, p128-132. 5p.
Publication Year :
2018

Abstract

We have been working on developing a low-cost tabletop NMR system. We reported that a field homogeneity as high as 50 ppm was achieved with a simple NMR magnet by employing two facing ferrite magnets with iron disks in between (Chonlathep et al., 2017). In this paper, we report two improvements added to our previous system: (1) an FPGA based signal processing unit to improve the S/N ratio and (2) a simple shimming mechanism to improve the field homogeneity. We obtained as high as 1 ppm field homogeneity in the best case. The signals from hydrogen nuclear spins in a methyl and carboxy group in acetic acid were resolved in NMR spectra. [ABSTRACT FROM AUTHOR]

Details

Language :
English
ISSN :
10907807
Volume :
294
Database :
Academic Search Index
Journal :
Journal of Magnetic Resonance
Publication Type :
Academic Journal
Accession number :
131091194
Full Text :
https://doi.org/10.1016/j.jmr.2018.07.003