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Three-dimensional interconnected Co(OH)2 nanosheets on Ti mesh as a highly sensitive electrochemical sensor for hydrazine detection.
- Source :
-
New Journal of Chemistry . 2/21/2019, Vol. 43 Issue 7, p3218-3225. 8p. - Publication Year :
- 2019
-
Abstract
- Three-dimensional interconnected Co(OH)2 nanosheets (Co(OH)2 NS) were electrodeposited onto a Ti mesh (TM) surface, which was demonstrated by XRD, Raman spectroscopy, XPS and SEM characterization. The electrochemical sensing performance of the Co(OH)2 NS/TM toward hydrazine was investigated by cyclic voltammetry and amperometric techniques in a 0.1 M NaOH aqueous solution. The as-prepared Co(OH)2 NS/TM with an electrodeposition time of 10 min exhibited prominent capacity to detect hydrazine with a wide linear range from 5 μM to 3.0 mM and limit of detection (LOD) of 1.98 μM. Co(OH)2 NS/TM electrodes also showed a high sensitivity of 2793.9 μA mM−1 cm−2, excellent selectivity, reproducibility, appreciable stability with a RSD less than 3.5%, as well as the high recovery of hydrazine in real samples, indicating its potential application in real sample analysis. [ABSTRACT FROM AUTHOR]
- Subjects :
- *HYDRAZINE
*ELECTROCHEMICAL analysis
*NANOSTRUCTURED materials
Subjects
Details
- Language :
- English
- ISSN :
- 11440546
- Volume :
- 43
- Issue :
- 7
- Database :
- Academic Search Index
- Journal :
- New Journal of Chemistry
- Publication Type :
- Academic Journal
- Accession number :
- 134648401
- Full Text :
- https://doi.org/10.1039/c8nj06008h