Local residual stresses and microstructure within recrystallizing grains in iron.

The intragranular strains and the microstructure within recrystallizing grains in single phase pure iron have been systematically studied in 3D using synchrotron micro-diffraction. In contradiction to common knowledge we observe that residual elastic strains of up to 1–2 × 10−3 are present in the recrystallizing grains. The local strain variations within individual grains can be similar in magnitude to those between different grains. The effects of processing parameters, including rolling reduction, recrystallized volume fraction, and cooling rate, as well as microstructural parameters, including grain size, orientation and internal misorientation, on the development of local residual elastic strains and microstructure have been quantified. It is suggested that the difference in local defect density between recrystallized grains and the surrounding deformed matrix, as well as the redistribution of medium to long-range residual stresses in the deformed grains, are the main reasons for the development of such strains in the recrystallized grains. The local residual stress levels are calculated and their possible impact on the mechanical properties and recrystallization processes are discussed. [Display omitted] • Local residual stresses in partially recrystallized iron have been mapped in 3D. • Residual elastic strains of up to 1–2 × 10−3 are present in recrystallizing grains. • Deviatoric strain components along different sample directions are different. • Mechanisms for the formation of local residual stresses in recrystallizing grains are clarified. • Importance of local residual stresses for recrystallization process is highlighted. [ABSTRACT FROM AUTHOR]