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Asimetrik Schiff Bazı ve Geçiş Metal Komplekslerinin Sentezi ve Karakterizasyonu.

Authors :
ÇAKRAN, Halide Sinem
DEMETGÜL, Cahit
Source :
Journal of the Institute of Science & Technology / Iğdır Üniversitesi Fen Bilimleri Enstitüsü Dergisi. Sep2022, Vol. 12 Issue 3, p1743-1757. 15p.
Publication Year :
2022

Abstract

In this study, firstly, monoimine compound (H3A) was synthesized from the condensation of 2-aminobenzylamine and 1'-hydroxy-2-acetonaphthone which is a ketone derivative. Asymmetric Schiff base (H2L) was synthesized as a result of the condensation of the obtained H3A and 5-bromosalicylaldehyde. After that, the synthesis and characterization of the Cu(II), Ni(II), Co(II) and Fe(III) complexes of the synthesized H2L compound were carried out. The proposed structures of Schiff bases and its metal complexes were elucidated using analytical and spectroscopic (UV-Vis, FTIR, elemental, 13C and ¹H NMR, LC-MS, ICP-AES, magnetic susceptibility, molar conductivity, and TG-DTA) methods. [ABSTRACT FROM AUTHOR]

Details

Language :
Turkish
ISSN :
21460574
Volume :
12
Issue :
3
Database :
Academic Search Index
Journal :
Journal of the Institute of Science & Technology / Iğdır Üniversitesi Fen Bilimleri Enstitüsü Dergisi
Publication Type :
Academic Journal
Accession number :
159590846
Full Text :
https://doi.org/10.21597/jist.1107255