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THE EFFECT OF DIFFERENT TYPES OF SOLVENTS ON MORPHOLOGY OF CARBON-MODIFIED TIO2/H-ZSM-5 COMPOSITE.

Authors :
Hartanto, Djoko
Indrawan, A. K.
Iryani, Ani
Rosyidah, Afifah
Rozafia, A. I.
Widyanto, A. R.
Source :
Rasayan Journal of Chemistry. Oct-Dec2022, Vol. 15 Issue 4, p2879-2884. 6p.
Publication Year :
2022

Abstract

This study aims to investigate the effects of different solvents (isopropanol, benzene, and toluene) on the synthesis of carbon-modified TiO2/H-ZSM-5 composites. Carbon-modified TiO2/H-ZSM-5 composites were characterized by FTIR, XRD, and SEM. XRD analysis revealed that the TiO2 peaks at 2 = 25.3, 37.8, and 48.2° had distinct characteristics. FTIR analysis revealed that I-ZTC, B-ZTC, and T-ZTC had comparable absorption bands to ZSM-5 at 3464, 1639, 1222, 1097, and 545 cm-1, respectively. Additionally, the FTIR data revealed that I-ZTC, B-ZTC, and T-ZTC all display absorption bands around the wavenumber 450 cm-1, indicating the Ti-O bond's stretching vibration. Additionally, SEM-EDX analysis revealed that Ti was more evenly distributed on the surface of T-ZTC than on the surfaces of B-ZTC and I-ZTC. It was shown that the solvent's polarity has an effect on TiO2 dispersion. A less polar solvent disperses TiO2 more effectively. In terms of TiO2 dispersion, toluene was the preferable solvent for the production of carbon-modified TiO2/H-ZSM-5. [ABSTRACT FROM AUTHOR]

Details

Language :
English
ISSN :
09741496
Volume :
15
Issue :
4
Database :
Academic Search Index
Journal :
Rasayan Journal of Chemistry
Publication Type :
Academic Journal
Accession number :
161351376
Full Text :
https://doi.org/10.31788/RJC.2022.1547013