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Present Status of 920 MHz High-Resolution NMR Spectrometers.

Authors :
Kiyoshi, Tsukasa
Maeda, Hideaki
Kikuchi, Jun
Ito, Yutaka
Hirota, Hiroshi
Yokoyama, Shigeyuki
Ito, Satoshi
Miki, Takashi
Hamada, Mamoru
Ozaki, Osamu
Hayashi, Seiji
Kurihara, Noriaki
Suematsu, Hiroto
Yoshikawa, Masatoshi
Matsumoto, Shinji
Sato, Akio
Wada, Hitoshi
Source :
IEEE Transactions on Applied Superconductivity. Jun2004, Vol. 14 Issue 2, p1608-1612. 5p.
Publication Year :
2004

Abstract

The first 920 MHz high-resolution NMR (Nuclear Magnetic Resonance) magnet was successfully installed at the Tsukuba Magnet Laboratory of the National Institute for Materials Science. A persistent operation at 21.6 T has continued since April 2002 without any problems. Excellent field stability of 0.31 Hz/h was observed from December 2002 to January 2003. Since July 2002, the magnet was used as an essential part of the only 920 MHz high-resolution NMR spectrometer in the world. The signal-to-noise ratio of 0.1 % ethylbenzene using a proton-selective probe was as high as 2981. An HCN triple-resonance probe is now attached to the spectrometer to contribute to the National Project on Protein Structural and Functional Analysis in Japan. The completion of the second 920 MHz-class NMR spectrometer is scheduled for spring 2004. [ABSTRACT FROM AUTHOR]

Details

Language :
English
ISSN :
10518223
Volume :
14
Issue :
2
Database :
Academic Search Index
Journal :
IEEE Transactions on Applied Superconductivity
Publication Type :
Academic Journal
Accession number :
16274799
Full Text :
https://doi.org/10.1109/TASC.2004.831010