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Preparation, spectral analysis of a substituted phenyl acetanilide from aniline.

Authors :
Mir, M. Amin
Ashraf, M. Waqar
Andrews, Kim
Source :
AIP Conference Proceedings. 2024, Vol. 3122 Issue 1, p1-7. 7p.
Publication Year :
2024

Abstract

For the synthesis of acetanilide from aniline, magnesium sulfate-glacial acetic acid system is a safe, environmentally friendly, and reasonably priced catalyst. The procedure is quick, easy, and environmentally friendly, does not require hazardous acetic anhydride, and uses a catalyzed reaction in accordance with green chemistry principles. The technique is simple to use at the undergraduate level and might be used to acetylate primary and secondary amines on a large scale in industry. The crystal that was treated using the aforementioned approach underwent numerous characterisation analyses. The sample's crystalline nature was confirmed by the powder X-ray diffraction technique. The crystal's functional group was located via FT-IR spectrum analysis. UV-Visible investigations looked at the crystals' transparency and optical characteristics. Through differential thermal analysis and differential scanning calorimetry (DTA/DSC), the thermal stability of the formed crystal was analysed. To display the molecular structure, 1HNMR spectra was analysed. The crystal's band gap value supports the material's application-oriented features. [ABSTRACT FROM AUTHOR]

Details

Language :
English
ISSN :
0094243X
Volume :
3122
Issue :
1
Database :
Academic Search Index
Journal :
AIP Conference Proceedings
Publication Type :
Conference
Accession number :
177948513
Full Text :
https://doi.org/10.1063/5.0216052