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乙酸乙酯皂化反应和碘钟反应实验改进.

Authors :
张睿桐
曾志强
张晓光
Source :
University Chemistry. 2024, Vol. 39 Issue 8, p197-203. 7p.
Publication Year :
2024

Abstract

This study addresses issues such as low efficiency in maintaining a constant temperature, uneven temperature distribution, uneven mixture, uneven reaction, and large deviations in experimental data observed in the ethyl acetate saponification reaction and iodine clock reaction. To address these problems, improvements are made in two aspects: the reaction vessel and the mixing method of reactants. The use of a jacketed beaker paired with a reaction flask as the reaction vessel and a multi-site magnetic stirrer for rapid mixing of the reactants is proposed. This improvement ensures a uniform and stable temperature in the solution, enhances the uniform dispersion and rapid reaction of the reactants, and enables accurate measurements of solution conductivity and the time for color change. The obtained data provides accurate values for reaction order, rate constant, and activation energy. [ABSTRACT FROM AUTHOR]

Details

Language :
Chinese
ISSN :
10008438
Volume :
39
Issue :
8
Database :
Academic Search Index
Journal :
University Chemistry
Publication Type :
Academic Journal
Accession number :
179218513
Full Text :
https://doi.org/10.3866/PKU.DXHX202312004