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Synthesis and characterization of CdS/PVA nanocomposite films
- Source :
-
Applied Surface Science . Aug2007, Vol. 253 Issue 20, p8495-8499. 5p. - Publication Year :
- 2007
-
Abstract
- Abstract: A series CdS/PVA nanocomposite films with different amount of Cd salt have been prepared by means of the in situ synthesis method via the reaction of Cd2+-dispersed poly vinyl-alcohol (PVA) with H2S. The as-prepared films were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), ultraviolet-visible (UV–vis) absorption, photoluminescence (PL) spectra, Fourier transform infrared spectroscope (FTIR) and thermogravimetric analysis (TGA). The XRD results indicated the formation of CdS nanoparticles with hexagonal phase in the PVA matrix. The primary FTIR spectra of CdS/PVA nanocomposite in different processing stages have been discussed. The vibrational absorption peak of Cd 405cm−1 was observed, which further testified the generation of CdS nanoparticles. The TGA results showed incorporation of CdS nanoparticles significantly altered the thermal properties of PVA matrix. The photoluminescence and UV–vis spectroscopy revealed that the CdS/PVA films showed quantum confinement effect. [Copyright &y& Elsevier]
- Subjects :
- *THIN films
*CADMIUM
*SALT
*TRANSMISSION electron microscopy
Subjects
Details
- Language :
- English
- ISSN :
- 01694332
- Volume :
- 253
- Issue :
- 20
- Database :
- Academic Search Index
- Journal :
- Applied Surface Science
- Publication Type :
- Academic Journal
- Accession number :
- 26569434
- Full Text :
- https://doi.org/10.1016/j.apsusc.2007.04.020