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rac-12a,11b-Diphenyl-1,2,3,4,5,11-hexahydro-2,3,4a,5a,10a,11a-hexaazabenz[ f]indeno[2,1,8- ija]naphth[2,3- f]azulene-1,4,10-trione chloroform solvate.

Authors :
Sheng-Li Hu
Jian-Min Zhang
Gang Yan
Shuai Wang
Source :
Acta Crystallographica: Section E. Sep2007, Vol. 63 Issue 9, po3909-o3909. 1p. 5 Diagrams, 5 Charts.
Publication Year :
2007

Abstract

The title compound, C25H20N6O3·CHCl3, a rigid glycoluril derivative, is an intermediate for the synthesis of molecular tweezers. The crystal structure is stabilized by intermolecular C—H...O and N—H...O hydrogen bonds. The chloroform solvent molecule is disordered over two positions; the site occupancy factors are ca 0.89 and 0.11. [ABSTRACT FROM AUTHOR]

Details

Language :
English
ISSN :
16005368
Volume :
63
Issue :
9
Database :
Academic Search Index
Journal :
Acta Crystallographica: Section E
Publication Type :
Academic Journal
Accession number :
26597534
Full Text :
https://doi.org/10.1107/S1600536807041591