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Microwave-Assisted Dehalogenation of α-Haloketones by Zinc and Ammonium Chloride in Alcohol.
- Source :
-
Synthetic Communications . 2008, Vol. 38 Issue 4, p567-575. 9p. 6 Diagrams, 3 Charts. - Publication Year :
- 2008
-
Abstract
- The treatment of α-haloketones with 1.5 equiv. of Zn and 1 equiv. of NH4Cl in ethanol for 0.5 min gave the corresponding ketones with excellent yields under microwave irradiation. Vic-dibromides and 2,2-dibromoacetophenone can be efficiently debrominated to alkenes and acetophenones, respectively. [ABSTRACT FROM AUTHOR]
- Subjects :
- *OXO compounds
*ALCOHOL
*ZINC
*KETONES
*ALKENES
*ACETOPHENONE
Subjects
Details
- Language :
- English
- ISSN :
- 00397911
- Volume :
- 38
- Issue :
- 4
- Database :
- Academic Search Index
- Journal :
- Synthetic Communications
- Publication Type :
- Academic Journal
- Accession number :
- 29343804
- Full Text :
- https://doi.org/10.1080/00397910701797889