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Microwave Promoted Environmentally Benign Synthesis of 2-Aminobenzothiazoles and Their Urea Derivatives.
- Source :
-
Phosphorus, Sulfur & Silicon & the Related Elements . May2008, Vol. 183 Issue 5, p1124-1133. 10p. 2 Diagrams, 1 Chart. - Publication Year :
- 2008
-
Abstract
- 2-Aminobenzothiazoles were efficiently synthesized using stable, crystalline tetrabutylammonium tribromide instead of toxic, corrosive liquid bromine under solvent-free and microwave irradiation condition. Furthermore, benzothiazol-2-ylureas were synthesized in good to high yield by reactions of 2-aminobenzothiazoles with N-trichloroacetanilides, which were used as a substitute for toxic, unstable isocyanates, under microwave irradiation condition. This protocol has advantages of no utilization of hazardous chemicals, rapid reaction rate, high yield, and easy work-up procedure. [ABSTRACT FROM AUTHOR]
- Subjects :
- *MICROWAVES
*ELECTRIC waves
*THIAZOLES
*AZOLES
*ORGANOSULFUR compounds
*UREA
Subjects
Details
- Language :
- English
- ISSN :
- 10426507
- Volume :
- 183
- Issue :
- 5
- Database :
- Academic Search Index
- Journal :
- Phosphorus, Sulfur & Silicon & the Related Elements
- Publication Type :
- Academic Journal
- Accession number :
- 31963516
- Full Text :
- https://doi.org/10.1080/10426500701578506