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Solubilities of Diphenylphosphinic Acid in Selected Solvents.

Authors :
Gai-Qing Zhang
Rui-Lan Fan
Xian-Zhao Shao
Xiao-Fang Wang
Li-Sheng Wang
Source :
Journal of Chemical & Engineering Data. Apr2008, Vol. 53 Issue 5, p1192-1195. 4p.
Publication Year :
2008

Abstract

Diphenylphosphinic acid (DPPA) was synthesized and characterized by infrared spectroscopy (IR), nuclear magnetic resonance ( 1H NMR), mass spectroscopy (MS), and elemental analysis. The melting point and the enthalpy of fusion of DPPA were measured by a differential scanning calorimeter (DSC), and the thermal stability of DPPA was measured by thermogravimetric analysis (TGA). The solubility data of DPPA in nine solvents were measured and correlated with an empirical equation. The estimated uncertainty of all the solubility values based on error analysis and repeated observations was within 2.0 %. [ABSTRACT FROM AUTHOR]

Details

Language :
English
ISSN :
00219568
Volume :
53
Issue :
5
Database :
Academic Search Index
Journal :
Journal of Chemical & Engineering Data
Publication Type :
Academic Journal
Accession number :
33003573
Full Text :
https://doi.org/10.1021/je800049b