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New organotin complexes with trans(cis)-1,4-cyclohexanedicarboxylic acid: Synthesis, characterization and crystal structures of mononuclears, 2D network polymers and a tetratin macrocycle
- Source :
-
Inorganica Chimica Acta . Aug2009, Vol. 362 Issue 11, p4137-4144. 8p. - Publication Year :
- 2009
-
Abstract
- Abstract: A series of new organotin carboxylates have been synthesized by reactions of trans(cis)-1,4-cyclohexanedicarboxylic acid with triorganotin chloride and diorganotin dichloride. All the complexes were characterized by elemental analysis, IR, 1H NMR, 13C NMR, 119Sn NMR spectroscopy; furthermore, complexes 1, 3, 5, 8 and 9 were characterized by X-ray diffraction analyses. The structural analyses show that complex 1 possesses a monomer structure; complex 5 possesses a 1D zigzag chain structure; both the complexes 3 and 8 have 2D network structures and complex 9 has a tetratin 36-membered macrocyclic structure. [Copyright &y& Elsevier]
Details
- Language :
- English
- ISSN :
- 00201693
- Volume :
- 362
- Issue :
- 11
- Database :
- Academic Search Index
- Journal :
- Inorganica Chimica Acta
- Publication Type :
- Academic Journal
- Accession number :
- 43618618
- Full Text :
- https://doi.org/10.1016/j.ica.2009.06.016