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Synthesis and Characterization of Mesoporous Alumina-Zirconia as Catalyst Support for Suzuki Coupling Reaction.
- Source :
-
Tenside Surfactants Detergents . Jan/Feb2012, Vol. 49 Issue 1, p43-47. 5p. - Publication Year :
- 2012
-
Abstract
- One pot facile synthesis of ordered mesoporous alumina-supported zirconia with high thermal stability and large pore sizes by evaporation-induced method was systematically investigated. The strategy based on a sol-gel process associated with nonionic triblock copolymers PPO-PEO-PPO as templates in ethanolic solution. Small-angle XRD, TEM, and nitrogen adsorption and de-sorption results showed that these composites possessed an ordered 2D hexagonal mesostructure, resisted to high temperature up to 1000 °C, and had large surface areas and narrow pore-size distributions. Loaded with palladium, the mesoporous alumina-zirconia composite exhibited high catalytic activity in Suzuki coupling of 2-bromotoluene with phenylboronic acid. [ABSTRACT FROM AUTHOR]
Details
- Language :
- English
- ISSN :
- 09323414
- Volume :
- 49
- Issue :
- 1
- Database :
- Academic Search Index
- Journal :
- Tenside Surfactants Detergents
- Publication Type :
- Academic Journal
- Accession number :
- 79963501
- Full Text :
- https://doi.org/10.3139/113.110165