Magnetic domain observation of Nd-Fe-B magnets with submicron-sized grains by high-resolution Kerr microscopy.

A Kerr microscope that uses UV light for high-resolution observation of magnetic domains was developed, and the domain structure and magnetization process of hot-pressed magnets prepared from hydrogenation-disproportionation-desorption-recombination (HDDR) processed powders were examined. This microscope is capable of distinguishing nanometer-sized domain patterns. The coercivity of the hot-pressed HDDR magnet depends on the area of magnetization reversal during a reversal process. Magnetization reversal occurs simultaneously in a few grains in a low-coercivity magnet because the Nd-rich phase along the grain boundaries is absent. In contrast, in a high-coercivity magnet, magnetization reversal in a grain independently occurs because of an adequate Nd-rich phase along the grain boundaries. It follows that the high coercivity of an HDDR powder compacted by hot pressing is due to domain wall pinning at the grain boundaries. [ABSTRACT FROM AUTHOR]