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Sensitivity and Resolution Enhanced Solid-State NMR for Paramagnetic Systems and Biomolecules under Very Fast Magic Angle Spinning.

Authors :
Parthasarathy, Sudhakar
Nishiyama, Yusuke
Ishii, Yoshitaka
Source :
Accounts of Chemical Research. Sep2013, Vol. 46 Issue 9, p2127-2135. 9p.
Publication Year :
2013

Abstract

Recent research in fast magic angle spinning (MAS) methods has drasticallyimproved the resolution and sensitivity of NMR spectroscopy of biomolecules and materials in solids. In this Account, we summarize recent and ongoing developments in this area by presenting 13C and 1H solid-state NMR (SSNMR) studies on paramagnetic systems and biomolecules under fast MAS from our laboratories. [ABSTRACT FROM AUTHOR]

Details

Language :
English
ISSN :
00014842
Volume :
46
Issue :
9
Database :
Academic Search Index
Journal :
Accounts of Chemical Research
Publication Type :
Academic Journal
Accession number :
90292107
Full Text :
https://doi.org/10.1021/ar4000482