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[Study on the spectrophotometric determination of microamounts of iron with 1-(2-pyridylazo)-2-naphthol-6-sulphonic acid].
- Source :
-
Wei sheng yan jiu = Journal of hygiene research [Wei Sheng Yan Jiu] 2002 Jun; Vol. 31 (3), pp. 210-1. - Publication Year :
- 2002
-
Abstract
- A new spectrophotometric method has been developed for the highly selective determination of Fe2+ with 1-(2-pyridylazo)-2-naphthol-6-sulphonic Acid. At pH 4.0, Fe2+ an be selectively determined at the wavelength of 760 nm. The calibration curve is liner in a concentration range of 0-10 micrograms/10 ml, relative coefficient is 0.9997, the apparent molar absorptivity is 1.57 x 104 L.mol-1.cm-1, RSD of within-run and between-day were 1.66% and 2.51%, the average rate of recovery 101.1%. The method has been applied to the direct determination of iron in milk powder, common coexistent substances don't interfere with the determination.
Details
- Language :
- Chinese
- ISSN :
- 1000-8020
- Volume :
- 31
- Issue :
- 3
- Database :
- MEDLINE
- Journal :
- Wei sheng yan jiu = Journal of hygiene research
- Publication Type :
- Academic Journal
- Accession number :
- 12545766