Back to Search
Start Over
Structural and optical characterization of pyrolytic carbon derived from novolac resin.
- Source :
-
Analytical and bioanalytical chemistry [Anal Bioanal Chem] 2004 Jul; Vol. 379 (5-6), pp. 788-91. Date of Electronic Publication: 2004 Jan 21. - Publication Year :
- 2004
-
Abstract
- The structural and optical properties of technologically interesting pyrolytic carbons formed from cured novolac resin and cured novolac/biomass composites were studied by X-Ray Diffraction Analysis (XRD), and Fourier Transform Infrared (FTIR), Raman and Photoluminescence (PL) spectroscopy. Pyrolysis of the cured materials took place at temperatures in the range 400-1000 degrees C. The most important weight loss, shrinkage and structural changes of pyrolyzed composites are observed at temperatures up to 600 degrees C due to the olive stone component. In the same temperature range, the changes in pyrolyzed novolac are smaller. The spectroscopic analysis shows that novolac pyrolyzed up to 900 ( degrees )C has less defects and disorder than the composites. However, above 900 ( degrees )C, pyrolyzed novolac becomes more disordered compared to the pyrolyzed composites. It is concluded that partial replacement of novolac by olive stone in the composite materials leads to the formation of a low cost, good quality product.
Details
- Language :
- English
- ISSN :
- 1618-2642
- Volume :
- 379
- Issue :
- 5-6
- Database :
- MEDLINE
- Journal :
- Analytical and bioanalytical chemistry
- Publication Type :
- Academic Journal
- Accession number :
- 14735272
- Full Text :
- https://doi.org/10.1007/s00216-003-2453-5