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Synthesis and structure of all-syn-1,2,3,4-tetrafluorocyclohexane.

Authors :
Durie AJ
Slawin AM
Lebl T
Kirsch P
O'Hagan D
Source :
Chemical communications (Cambridge, England) [Chem Commun (Camb)] 2011 Aug 07; Vol. 47 (29), pp. 8265-7. Date of Electronic Publication: 2011 Jun 28.
Publication Year :
2011

Abstract

Preparation of the all-syn isomer of 1,2,3,4-tetrafluorocyclohexane is reported; X-ray structural studies shows a conformation with two of the C-F bonds oriented 1,3-diaxial to each other and (19)F-NMR reveals a through space diaxial (4)J(FF) coupling constant of 29 Hz.

Details

Language :
English
ISSN :
1364-548X
Volume :
47
Issue :
29
Database :
MEDLINE
Journal :
Chemical communications (Cambridge, England)
Publication Type :
Academic Journal
Accession number :
21709894
Full Text :
https://doi.org/10.1039/c1cc13016a