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In-cell solid-state NMR as a tool to study proteins in large complexes.

Authors :
Reckel S
Lopez JJ
Löhr F
Glaubitz C
Dötsch V
Source :
Chembiochem : a European journal of chemical biology [Chembiochem] 2012 Mar 05; Vol. 13 (4), pp. 534-7. Date of Electronic Publication: 2012 Feb 01.
Publication Year :
2012

Abstract

A major limitation of solution NMR is molecular tumbling, which is often too slow for detection. Here we demonstrate that solid-state NMR spectroscopy in combination with flash freezing of cells can be used to detect proteins in the cellular environment and provides information on backbone chemical shifts.<br /> (Copyright © 2012 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.)

Details

Language :
English
ISSN :
1439-7633
Volume :
13
Issue :
4
Database :
MEDLINE
Journal :
Chembiochem : a European journal of chemical biology
Publication Type :
Academic Journal
Accession number :
22298299
Full Text :
https://doi.org/10.1002/cbic.201100721