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Near-IR absorbing nickel(II) porphyrinoids prepared by regioselective insertion of silylenes into antiaromatic nickel(II) norcorrole.

Authors :
Fukuoka T
Uchida K
Sung YM
Shin JY
Ishida S
Lim JM
Hiroto S
Furukawa K
Kim D
Iwamoto T
Shinokubo H
Source :
Angewandte Chemie (International ed. in English) [Angew Chem Int Ed Engl] 2014 Feb 03; Vol. 53 (6), pp. 1506-9. Date of Electronic Publication: 2014 Jan 28.
Publication Year :
2014

Abstract

The treatment of an antiaromatic norcorrole Ni(II) complex with a kinetically stabilized silylene provided ring-expansion products in excellent yields through the highly regio- and stereoselective insertion into the β-β pyrrolic CC bonds. The resultant Ni(II) porphyrinoid monoinsertion product exhibited relatively strong near-IR absorption bands due to the small HOMO-LUMO gap in spite of the disrupted cyclic π-conjugation by the silicon atom.<br /> (Copyright © 2014 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.)

Details

Language :
English
ISSN :
1521-3773
Volume :
53
Issue :
6
Database :
MEDLINE
Journal :
Angewandte Chemie (International ed. in English)
Publication Type :
Academic Journal
Accession number :
24474697
Full Text :
https://doi.org/10.1002/anie.201309921