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4-Hy-droxy-3-meth-oxy-benzaldehyde 4-phenyl-thio-semicarbazone.

Authors :
de Oliveira AB
Feitosa BR
Näther C
Jess I
Source :
Acta crystallographica. Section E, Structure reports online [Acta Crystallogr Sect E Struct Rep Online] 2014 Feb 12; Vol. 70 (Pt 3), pp. o278. Date of Electronic Publication: 2014 Feb 12 (Print Publication: 2014).
Publication Year :
2014

Abstract

In the title compound, C15H15N3O2S, the central C-N-N-C unit has an anti conformation [torsion angle = -170.17 (15)°]. The phenyl substituent is oriented perpendicular to this unit [dihedral angle of 89.2 (1)°], whereas the substituted ring is rotated out of this plane by only 18.86 (17)°. In the crystal, mol-ecules are linked by pairs of N-H⋯S hydrogen bonds into inversion dimers that are further connected via N-H⋯O and O-H⋯S hydrogen bonds into a three-dimensional network.

Details

Language :
English
ISSN :
1600-5368
Volume :
70
Issue :
Pt 3
Database :
MEDLINE
Journal :
Acta crystallographica. Section E, Structure reports online
Publication Type :
Academic Journal
Accession number :
24764990
Full Text :
https://doi.org/10.1107/S1600536814002773