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An efficient one-pot four-segment condensation method for protein chemical synthesis.

Authors :
Tang S
Si YY
Wang ZP
Mei KR
Chen X
Cheng JY
Zheng JS
Liu L
Source :
Angewandte Chemie (International ed. in English) [Angew Chem Int Ed Engl] 2015 May 04; Vol. 54 (19), pp. 5713-7. Date of Electronic Publication: 2015 Mar 13.
Publication Year :
2015

Abstract

Successive peptide ligation using a one-pot method can improve the efficiency of protein chemical synthesis. Although one-pot three-segment ligation has enjoyed widespread application, a robust method for one-pot four-segment ligation had to date remained undeveloped. Herein we report a new one-pot multisegment peptide ligation method that can be used to condense up to four segments with operational simplicity and high efficiency. Its practicality is demonstrated by the one-pot four-segment synthesis of a plant protein, crambin, and a human chemokine, hCCL21.<br /> (© 2015 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.)

Details

Language :
English
ISSN :
1521-3773
Volume :
54
Issue :
19
Database :
MEDLINE
Journal :
Angewandte Chemie (International ed. in English)
Publication Type :
Academic Journal
Accession number :
25772600
Full Text :
https://doi.org/10.1002/anie.201500051