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Nanocrystal size distribution analysis from transmission electron microscopy images.

Authors :
van Sebille M
van der Maaten LJ
Xie L
Jarolimek K
Santbergen R
van Swaaij RA
Leifer K
Zeman M
Source :
Nanoscale [Nanoscale] 2015 Dec 28; Vol. 7 (48), pp. 20593-606. Date of Electronic Publication: 2015 Nov 23.
Publication Year :
2015

Abstract

We propose a method, with minimal bias caused by user input, to quickly detect and measure the nanocrystal size distribution from transmission electron microscopy (TEM) images using a combination of Laplacian of Gaussian filters and non-maximum suppression. We demonstrate the proposed method on bright-field TEM images of an a-SiC:H sample containing embedded silicon nanocrystals with varying magnifications and we compare the accuracy and speed with size distributions obtained by manual measurements, a thresholding method and PEBBLES. Finally, we analytically consider the error induced by slicing nanocrystals during TEM sample preparation on the measured nanocrystal size distribution and formulate an equation to correct this effect.

Details

Language :
English
ISSN :
2040-3372
Volume :
7
Issue :
48
Database :
MEDLINE
Journal :
Nanoscale
Publication Type :
Academic Journal
Accession number :
26593390
Full Text :
https://doi.org/10.1039/c5nr06292f