Back to Search Start Over

Low magnification differential phase contrast imaging of electric fields in crystals with fine electron probes.

Authors :
Taplin DJ
Shibata N
Weyland M
Findlay SD
Source :
Ultramicroscopy [Ultramicroscopy] 2016 Oct; Vol. 169, pp. 69-79. Date of Electronic Publication: 2016 Jul 05.
Publication Year :
2016

Abstract

To correlate atomistic structure with longer range electric field distribution within materials, it is necessary to use atomically fine electron probes and specimens in on-axis orientation. However, electric field mapping via low magnification differential phase contrast imaging under these conditions raises challenges: electron scattering tends to reduce the beam deflection due to the electric field strength from what simple models predict, and other effects, most notably crystal mistilt, can lead to asymmetric intensity redistribution in the diffraction pattern which is difficult to distinguish from that produced by long range electric fields. Using electron scattering simulations, we explore the effects of such factors on the reliable interpretation and measurement of electric field distributions. In addition to these limitations of principle, some limitations of practice when seeking to perform such measurements using segmented detector systems are also discussed.<br /> (Copyright © 2016 Elsevier B.V. All rights reserved.)

Details

Language :
English
ISSN :
1879-2723
Volume :
169
Database :
MEDLINE
Journal :
Ultramicroscopy
Publication Type :
Academic Journal
Accession number :
27449276
Full Text :
https://doi.org/10.1016/j.ultramic.2016.07.010