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Metal-Free Radical Oxidative Cyclization of o-Azidoaryl Acetylenic Ketones with Sulfinic Acids To Access Sulfone-Containing 4-Quinolones.

Authors :
Zhou N
Yan Z
Zhang H
Wu Z
Zhu C
Source :
The Journal of organic chemistry [J Org Chem] 2016 Dec 16; Vol. 81 (24), pp. 12181-12188. Date of Electronic Publication: 2016 Dec 06.
Publication Year :
2016

Abstract

A novel one-pot synthesis of sulfone-containing 4-quinolones with easily available sulfinic acids as sulfonylating precursors is described. This reaction is characterized by mild reaction conditions, high functional-group tolerance and amenability to gram-scale synthesis.

Details

Language :
English
ISSN :
1520-6904
Volume :
81
Issue :
24
Database :
MEDLINE
Journal :
The Journal of organic chemistry
Publication Type :
Academic Journal
Accession number :
27978760
Full Text :
https://doi.org/10.1021/acs.joc.6b01847