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Characterization of the Materials Synthesized by High Pressure-High Temperature Treatment of a Polymer Derived t-BC₂N Ceramic.
- Source :
-
Materials (Basel, Switzerland) [Materials (Basel)] 2011 Nov 29; Vol. 4 (12), pp. 2061-2072. Date of Electronic Publication: 2011 Nov 29. - Publication Year :
- 2011
-
Abstract
- Bulk B-C-N materials were synthesized under static high thermobaric conditions (20 GPa and 2,000 °C) in a multianvil apparatus from a polymer derived t-BC <subscript>1.97</subscript> N ceramic. The bulk samples were characterised using X-ray synchrotron radiation and analytical transmission electron microscopy in combination with electron energy loss spectroscopy. Polycrystalline B-C-N materials with a cubic type structure were formed under the applied reaction conditions, but the formation of a ternary cubic diamond-like c-BC₂N compound, could not be unambiguously confirmed.
Details
- Language :
- English
- ISSN :
- 1996-1944
- Volume :
- 4
- Issue :
- 12
- Database :
- MEDLINE
- Journal :
- Materials (Basel, Switzerland)
- Publication Type :
- Academic Journal
- Accession number :
- 28824124
- Full Text :
- https://doi.org/10.3390/ma4122061