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Isomer of linker for NU-1000 yields a new she-type, catalytic, and hierarchically porous, Zr-based metal-organic framework.

Authors :
Lu Z
Wang R
Liao Y
Farha OK
Bi W
Sheridan TR
Zhang K
Duan J
Liu J
Hupp JT
Source :
Chemical communications (Cambridge, England) [Chem Commun (Camb)] 2021 Apr 14; Vol. 57 (29), pp. 3571-3574. Date of Electronic Publication: 2021 Mar 11.
Publication Year :
2021

Abstract

The well-known MOF (metal-organic framework) linker tetrakis(p-benzoate)pyrene (TBAPy <superscript>4-</superscript> ) lacks steric hindrance between its benzoates. Changing the 1,3,6,8-siting of benzoates in TBAPy <superscript>4-</superscript> to 4,5,9,10-siting introduces substantial steric hindrance and, in turn, enables the synthesis of a new hierarchically porous, she-type MOF Zr <subscript>6</subscript> (μ <subscript>3</subscript> -O) <subscript>4</subscript> (μ <subscript>3</subscript> -OH) <subscript>4</subscript> (C <subscript>6</subscript> H <subscript>5</subscript> COO) <subscript>3</subscript> (COO) <subscript>3</subscript> (TBAPy-2) <subscript>3/2</subscript> (NU-601), where TBAPy-2 <superscript>4-</superscript> is the 4,5,9,10 isomer of TBAPy <superscript>4-</superscript> . NU-601 shows high catalytic activity for degradative hydrolysis of a simulant for G-type fluoro-phosphorus nerve agents.

Details

Language :
English
ISSN :
1364-548X
Volume :
57
Issue :
29
Database :
MEDLINE
Journal :
Chemical communications (Cambridge, England)
Publication Type :
Academic Journal
Accession number :
33704273
Full Text :
https://doi.org/10.1039/d0cc07974j