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Acid-Free Copper-Catalyzed Electrophilic Nitration of Electron-Rich Arenes with Guanidine Nitrate.

Authors :
Li WP
Cheng G
Li SY
Lin CZ
Guan XY
Bing DX
Cao J
Zhu D
Deng QH
Source :
The Journal of organic chemistry [J Org Chem] 2022 Mar 04; Vol. 87 (5), pp. 3834-3840. Date of Electronic Publication: 2022 Feb 16.
Publication Year :
2022

Abstract

A practical copper-catalyzed nitration of electron-rich arenes with trimethylsilyl chloride and guanidine nitrate is reported. A variety of nitrated products were generated in moderate to excellent yields (32-99%) at ambient temperature under acid-free, open-flask, and operationally simple conditions.

Details

Language :
English
ISSN :
1520-6904
Volume :
87
Issue :
5
Database :
MEDLINE
Journal :
The Journal of organic chemistry
Publication Type :
Academic Journal
Accession number :
35168320
Full Text :
https://doi.org/10.1021/acs.joc.1c03020