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Modulated self-assembly of three flexible Cr(III) PCPs for SO 2 adsorption and detection.

Authors :
López-Cervantes VB
Bara D
Yañez-Aulestia A
Martínez-Ahumada E
López-Olvera A
Amador-Sánchez YA
Solis-Ibarra D
Sánchez-González E
Ibarra IA
Forgan RS
Source :
Chemical communications (Cambridge, England) [Chem Commun (Camb)] 2023 Jun 27; Vol. 59 (52), pp. 8115-8118. Date of Electronic Publication: 2023 Jun 27.
Publication Year :
2023

Abstract

Modulated self-assembly protocols are used to develop facile, HF-free syntheses of the archetypal flexible PCP, MIL-53(Cr), and novel isoreticular analogues MIL-53(Cr)-Br and MIL-53(Cr)-NO <subscript>2</subscript> . All three PCPs show good SO <subscript>2</subscript> uptake (298 K, 1 bar) and high chemical stabilities against dry and wet SO <subscript>2</subscript> . Solid-state photoluminescence spectroscopy indicates all three PCPs exhibit turn-off sensing of SO <subscript>2</subscript> , in particular MIL-53(Cr)-Br, which shows a 2.7-fold decrease in emission on exposure to SO <subscript>2</subscript> at room temperature, indicating potential sensing applications.

Details

Language :
English
ISSN :
1364-548X
Volume :
59
Issue :
52
Database :
MEDLINE
Journal :
Chemical communications (Cambridge, England)
Publication Type :
Academic Journal
Accession number :
37306073
Full Text :
https://doi.org/10.1039/d3cc01685d