Back to Search Start Over

Development of analysis method for m-xylenediamine as aldehyde scavenger using HPLC–PDA: m-xylenediamine determination by HPLC-PDA: J.-W. Shim et al.

Authors :
Shim, Ji-Won
Kim, Sun-Hae
Shin, Han-Seung
Shin, Jae-Wook
Source :
Food Science & Biotechnology; Jan2025, Vol. 34 Issue 1, p95-102, 8p
Publication Year :
2025

Abstract

The objective of this study was to develop an analytical method for m-xylenediamine (m-XDA), an aldehyde scavenger, in various food simulants and food matrices. The analysis was performed using HPLC–UV (270 nm) with a Capcell pak MGII C18 column (4.6 × 250 mm, 5 μm). The method validation encompassed evaluations of specificity, linearity, accuracy, precision, limit of detection (LOD), and limit of quantification (LOQ) across five food simulants and six food matrices. In the calibration curve range of 1–100 μg/mL, excellent linearity was observed with R<superscript>2</superscript> ≥ 0.9992. The accuracy and precision were within the ranges of 86.4–98.6% and 0.7–2.9 relative standard deviation (RSD%), respectively. The LOD and LOQ were in the ranges of 0.26–0.56 μg/mL and 0.79–1.71 μg/mL, respectively. The significance lies in the development of analysis methods for each food matrix, not only for smart packaging simulant analysis. This research makes it well-suited for smart packaging safety management. [ABSTRACT FROM AUTHOR]

Details

Language :
English
ISSN :
12267708
Volume :
34
Issue :
1
Database :
Complementary Index
Journal :
Food Science & Biotechnology
Publication Type :
Academic Journal
Accession number :
182074235
Full Text :
https://doi.org/10.1007/s10068-024-01646-5