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Facile Synthesis of 2‐Alkylthio‐5,5‐dimethyl‐4H‐imidazol‐4‐ones.

Authors :
Yuan, Ju‐Zhen
Wei, Jia‐Jia
Ding, Ming‐Wu
Source :
Synthetic Communications; 2006, Vol. 36 Issue 19, p2921-2925, 4p, 2 Diagrams
Publication Year :
2006

Abstract

The isothiocyanate 3, obtained from aza‐Wittig reaction of iminophosphorane 2 with CS2, reacts with phenylhydrazine to give thiosemicarbazide 4. Reactions of 4 with alkyl halides in the presence of K2CO3 directly provided 2‐alkylthio‐4H‐imidazol‐4‐ones 6 in good yields. [ABSTRACT FROM AUTHOR]

Details

Language :
English
ISSN :
00397911
Volume :
36
Issue :
19
Database :
Complementary Index
Journal :
Synthetic Communications
Publication Type :
Academic Journal
Accession number :
22692792
Full Text :
https://doi.org/10.1080/00397910600772959