Synthesis and characterization of some di- and triorganotin (IV) complexes of new Schiff base Using Green methodology.

Authors :: Kaur, Harminder
Kapila, Akanksh
Puri, Jugal Kishore
Singla, Anita
Source :: Annual International Conference on Chemistry, Chemical Engineering & Chemical Process; Feb2013, p103-107, 5p
Publication Year :: 2013
Abstract: A new Schiff base was prepared from o-vanillin and acetazolamide followed by synthesis of di- and triorganotin(IV) complexes of the general formula R<subscript>n</subscript>Sn(L)<subscript>m</subscript> and R'<subscript>n</subscript>Sn(L)<subscript>m</subscript> [R = n-Bu, n = 2, m = 2; R' = n-?u, n = 3, m = 1; HL =Schiff base| by green methodology using microwaves. The synthesized complexes were characterized by elemental analysis and UV-Visible, IR and multinuclear (¹H, <superscript>13</superscript>C, <superscript>119</superscript>Sn) NMR Spectroscopic studies. [ABSTRACT FROM AUTHOR]

Subjects :: ORGANOTIN compounds
CHEMICAL synthesis
METAL complexes
VANILLIN
ACETAZOLAMIDE
NUCLEAR magnetic resonance spectroscopy

Language :: English
ISSN :: 23013761
Database :: Complementary Index
Journal :: Annual International Conference on Chemistry, Chemical Engineering & Chemical Process
Publication Type :: Conference
Accession number :: 92982019
Full Text :: https://doi.org/10.5176/2301-3761_CCECP.24

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