Solid-Phase Synthesis of Core 8 O-Glycan-Linked MUC5AC Glycopeptide.

Studies the solid-phase synthesis of benzyl-protected disaccharide building blocks of core 8 O-glycan protein for glycopeptide by two glycosidation reactions with the glycosyl fluoride method. Separation of the synthetic glycopeptide from the resin with reagent K; Use of the synthetic sample as a suitable standard in studies of the physicochemical or immunochemical characterization of mucin glycoforms.