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Polymer-Supported O-Methylisourea:  A New Reagent for the O-Methylation of Carboxylic Acids

Authors :
Crosignani, S.
White, P. D.
Linclau, B.
Source :
Organic Letters; March 2002, Vol. 4 Issue: 6 p1035-1037, 3p
Publication Year :
2002

Abstract

<UFIGR ID="ol025633sn00001">A solid-supported O-methylisourea reagent has been prepared in one step starting from commercially available solid-supported carbodiimide. The isourea reagent has been successfully used for the preparation of methyl esters from the corresponding carboxylic acids. The crude products obtained after resin filtration and solvent evaporation are generally obtained in >98% purity.

Details

Language :
English
ISSN :
15237060 and 15237052
Volume :
4
Issue :
6
Database :
Supplemental Index
Journal :
Organic Letters
Publication Type :
Periodical
Accession number :
ejs2072047
Full Text :
https://doi.org/10.1021/ol025633s