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CARBON-13 NMR STUDY OF AN INTERMEDIATE COMPLEX IN HYDROESTERIFICATION OF OLEFINS

Authors :
Shin, Shigemitsu
Matsuda, Akio
Nakayama, Jun-ichi
Bando, Ken-ichiro
Source :
Chemistry Letters; February 1977, Vol. 6 Issue: 2 p115-118, 4p
Publication Year :
1977

Abstract

Reaction of a new hydroesterification catalyst H2Co3Py5(CO)9with 2-vinylpyridine yielded an alkylcobalt complex (Remark: Graphics omitted.), which is considered to be an intermediate complex in the hydroesterification of 2-vinylpyridine. The 13C-NMR parameters of the α- and β-methylene groups were δ=60.0 ppm (JC-H=147 Hz) and 37.4 ppm (132 Hz), respectively.

Details

Language :
English
ISSN :
03667022 and 13480715
Volume :
6
Issue :
2
Database :
Supplemental Index
Journal :
Chemistry Letters
Publication Type :
Periodical
Accession number :
ejs64675803
Full Text :
https://doi.org/10.1246/cl.1977.115