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Unexpected Formation of Osmium Carbyne and Vinylidene Complexes from the Reaction of OsCl2(PPh3)3 with HC⋮CCMe3

Authors :
Guochen Jia
Ting-Bin Wen
Zhong Yuan Zhou
Chak-Po Lau
Zhenyang Lin
Sheng-Yong Yang
Source :
Organometallics. 19:3757-3761
Publication Year :
2000
Publisher :
American Chemical Society (ACS), 2000.

Abstract

Treatment of OsCl2(PPh3)3 with HC⋮CCMe3produced a mixture of OsCl3(⋮CCH2CMe3)(PPh3)2 and OsCl(CCHCMe3)(C(C⋮CCMe3)CHCMe3)(PPh3)2. The structures of the new complexes have been confirmed by X-ray diffraction studies.

Details

ISSN :
15206041 and 02767333
Volume :
19
Database :
OpenAIRE
Journal :
Organometallics
Accession number :
edsair.doi...........040ef8183e125faf6bd76734b760b9c0
Full Text :
https://doi.org/10.1021/om000306e