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Determination of Nine Food Additives in Condiment by High Performance Liquid Chromatography

Authors :
Mao Zhang Guo
Zhong Qiang He
Zhong Ling Wu
Source :
Applied Mechanics and Materials. 140:302-308
Publication Year :
2011
Publisher :
Trans Tech Publications, Ltd., 2011.

Abstract

The HPLC method has been developed for the determination of nine food additives (acesulfame-potassium, benzoic acid, sodium saccharin, sorbic acid, dehydroacetic acid, aspartame, methylparaben, ethylparaben, propylparaben) in condiments. Samples were precipitated , tested by the reverse-phase high performance liquid chromatography instrument with photodiode array detector . All the compounds exhibited good linear relationship with the correlation coefficient from 0.9991 to 0.9998. The recoveries were range from 87.1% to 108.5 % with the RSD values from 1.61 % to 5.13 % at the spiked levels from 5 mg/kg to 250 mg/kg. The detection limits of the method were from 0.3 mg/kg to 2.0 mg/kg. It is a convenient, accurate and effective method to determine these additives in condiment.

Details

ISSN :
16627482
Volume :
140
Database :
OpenAIRE
Journal :
Applied Mechanics and Materials
Accession number :
edsair.doi...........29925d90203fca369ff35e58d4abb66b