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Convenient Synthesis of Dicyclohexyldithiophosphinic Acid
- Source :
- Synthetic Communications. 40:2036-2041
- Publication Year :
- 2010
- Publisher :
- Informa UK Limited, 2010.
-
Abstract
- Dicyclohexyldithiophosphinic acid was synthesized by a three-step strategy through the Grignard reaction of PSCl3 with cyclo-C6H11MgBr and the P-P bond-cleavage reaction of the intermediate. The 1H NMR data of ammonium dicyclohexyldithiophosphinate 4 and dicyclohexyldithiophosphinic acid 5 were characterized by 1H-1H correlation spectra.
Details
- ISSN :
- 15322432 and 00397911
- Volume :
- 40
- Database :
- OpenAIRE
- Journal :
- Synthetic Communications
- Accession number :
- edsair.doi...........29e5ef77d5e690571967dfdd5c6e5c20