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Focusing and polarized neutron small-angle scattering spectrometer (SANS-J-II). The challenge of observation over length scales from an ångström to a micrometre

Authors :
H. Sasao
Daisuke Yamaguchi
Hiroki Iwase
Hirohiko M. Shimizu
Ryuhei Motokawa
Takeji Hashimoto
Hirokazu Tanaka
Satoshi Koizumi
Takayuki Oku
Jun-ichi Suzuki
Source :
Journal of Applied Crystallography. 40:s474-s479
Publication Year :
2007
Publisher :
International Union of Crystallography (IUCr), 2007.

Abstract

SANS-J (a pinhole small-angle neutron scattering spectrometer at research reactor JRR3, Tokai, Japan) was reconstructed as a focusing and polarized neutron small-angle scattering spectrometer (SANS-J-II). By employing focusing lenses of a biconcave MgF2 crystal or of a sextupole permanent magnet and a high-resolution photomultiplier, the minimum accessible magnitude of the scattering vector qmin was improved from 3 × 10−3 A−1 to an ultra-small-angle scattering (USAS) of 3 × 10−4 A−1. Compared with a Bonse–Hart double-crystal method, the advantages of focusing USAS are the efficient detection of anisotropic USAS with an area detector, an improvement in q resolution Δq/q at conventional magnitudes of the scattering vector q ~ 10−3 A−1 and a gain in neutron flux in the conventional q region of q ~ 10−3 A−1.

Details

ISSN :
00218898
Volume :
40
Database :
OpenAIRE
Journal :
Journal of Applied Crystallography
Accession number :
edsair.doi...........3f927413310e5cb10e440c0d8f3eecaa
Full Text :
https://doi.org/10.1107/s0021889807014392