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X-ray crystal structure analysis of N'-acetyl-N'-phenyl-2-naphthohydrazide
- Source :
- European Journal of Chemistry. 13:253-258
- Publication Year :
- 2022
- Publisher :
- European Journal of Chemistry, 2022.
-
Abstract
- N'-Acetyl-N'-phenyl-2-naphthohydrazide, a biologically relevant organic molecule, was synthesized following a reported method and characterized based on its single X-ray crystallographic studies. The present manuscript deals with its detailed molecular interactions and X-ray crystal structure. Its space group is P-1 with the following unit cell parameters: a = 8.9164(7), b = 9.7058(9), c = 17.7384(12) Å, α = 88.308(7)°, β = 89.744(6)°, γ = 86.744(7)° and Z = 2. Crystal structure was solved by direct method and refined by full matrix least squares procedure to a final R value of 0.0580 and to a GOOF value of 1.066. The X-ray diffraction analyses showed that the asymmetric unit contains two crystallographically independent molecules. The crystal structure is stabilized by elaborate network of N-H···O and C-H···O hydrogen bonds along with C-H···π and π···π interactions to form supramolecular structures.
Details
- ISSN :
- 21532257 and 21532249
- Volume :
- 13
- Database :
- OpenAIRE
- Journal :
- European Journal of Chemistry
- Accession number :
- edsair.doi...........545dd4fdb832428e8c7112a5bd0fdf4a
- Full Text :
- https://doi.org/10.5155/eurjchem.13.3.253-258.2235