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Advanced high-temperature ultracentrifuge apparatus for mega-gravity materials science

Authors :
Shiro Shibasaki
Tsutomu Mashimo
Toyotaka Osakabe
Nobuo Mori
Masamichi Nishihara
Masanori Sueyoshi
Hirotaka Ihara
Koji Shibasaki
Xinsheng Huang
Masao Ono
Source :
Review of Scientific Instruments. 74:160-163
Publication Year :
2003
Publisher :
AIP Publishing, 2003.

Abstract

An ultracentrifuge apparatus, which can generate an ultra-strong gravitational field even >1 000 000 (1 million) G (1 G=9.8 m/s2) over a wide temperature range up to >500 °C with high stability control, was developed for new materials science research. The system consists of an air turbine motor with ceramic ball bearings and dumper section, a sample rotor with an outer diameter of up to 160 mm, a vacuum chamber, and a heating system. The nonbored rotor and the double-structural dumper bushing are used to raise the maximum rotational speed and to improve the stability. The samples can be heated by radiant heat. A maximum rotational speed of 190 000 rpm using a 70 mm diam rotor was recorded despite a short time where the maximum gravitational field was >1 2000 000 G. Long and high-temperature ultracentrifuge experiments using 70 and 80 mm diam rotors made of titanium alloy with rotational speeds of up to 170 000 rpm even at temperatures of over 200 °C for 100 h with ripples of

Details

ISSN :
10897623 and 00346748
Volume :
74
Database :
OpenAIRE
Journal :
Review of Scientific Instruments
Accession number :
edsair.doi...........5a9f556d4a3a0ab29c0bc6b8f3262700
Full Text :
https://doi.org/10.1063/1.1527718