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Modernization of the small-angle neutron scattering spectrometer SANS-U by upgrade to a focusing SANS spectrometer

Authors :
Mitsuhiro Shibayama
Hiroki Iwase
Hitoshi Endo
Masaki Katagiri
Source :
Journal of Applied Crystallography. 44:558-568
Publication Year :
2011
Publisher :
International Union of Crystallography (IUCr), 2011.

Abstract

The small-angle neutron scattering spectrometer SANS-U at the research reactor (JRR-3) of the Japan Atomic Energy Agency, Tokai, Japan, has been successfully upgraded. This major upgrade was undertaken in order to install a high-resolution position-sensitive detector consisting of a cross-wired position-sensitive photomultiplier tube combined with a ZnS/6LiF scintillator on the SANS-U spectrometer. Without changing the total length of the spectrometer, the aim was to extend the accessible low-Qlimit (Qis the magnitude of the scattering vector) and to shorten the measurement time by employing focusing small-angle neutron scattering (FSANS). By using both spherical MgF2biconcave lenses and the new high-resolution position-sensitive detector, the accessible low-Qlimit was extended from 2.5 × 10−3to 3.8 × 10−4 Å−1. As a result, SANS-U can continuously cover a wideQrange from 3.8 × 10−4to 0.35 Å−1with a wavelength of 7 Å. FSANS can be utilized not only to improve the accessible low-Qlimit but also to increase the intensity of incident neutrons passing through the sample in the conventionalQrange from 2.5 × 10−3to 0.35 Å−1. The use of `high-intensity' FSANS also allowed a reduction of the measuring time by approximately 1/3.16 by increasing the incident neutron intensity.

Details

ISSN :
00218898
Volume :
44
Database :
OpenAIRE
Journal :
Journal of Applied Crystallography
Accession number :
edsair.doi...........6cd42ea142c248cf4df76784b0b526c4
Full Text :
https://doi.org/10.1107/s0021889811007527