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Reduction of Ni(ACAC)2Under Carbonylative Conditions: A Suitable Procedure for Small Scale Production of Ni (CO)4
- Source :
- Synthetic Communications. 17:1149-1153
- Publication Year :
- 1987
- Publisher :
- Informa UK Limited, 1987.
-
Abstract
- Reduction of diluted solutions of anhydrous Ni(II) acetylacetonate in THF by reducing alkylating agents such as DIBAH, n-Bu Li or PrMgBr in the presence of carbon monoxide gave practically quantitative yields of Ni (CO)4.
Details
- ISSN :
- 15322432 and 00397911
- Volume :
- 17
- Database :
- OpenAIRE
- Journal :
- Synthetic Communications
- Accession number :
- edsair.doi...........872c6b762d97440716b0672a9375e8d5
- Full Text :
- https://doi.org/10.1080/00397918708063964