A new example of linear disiloxane: Synthesis and X-ray crystal structure of bis(2-silolyl)tetramethyldisiloxane

Authors :: Shigehiro Yamaguchi
Kohei Tamao
Motoo Shiro
Ren-Zhi Jin
Source :: Chemistry of Heterocyclic Compounds. 33:155-160
Publication Year :: 1997
Publisher :: Springer Science and Business Media LLC, 1997.
Abstract: Bis(2-silolyl)tetramethyldisiloxane has been obtained by an attempted Wurtz-type coupling of (2-silolyl)dimethylsilyl chloride using sodium metal, and its linear Si−O−Si geometry has been demonstrated by X-ray crystallography.

Subjects :: Chemistry
Organic Chemistry
X-ray
Crystal structure
Disiloxane
Chloride
Metal
Crystallography
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