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ChemInform Abstract: An Efficient Method for Preparation of Chiral Arylmenthol Glyoxylates

Authors :
José E. Rodríguez-Borges
Olga Caamaño
Xerardo García-Mera
José M. Blanco
Antonio R. Hergueta
Carmen López
Franco Fernández
Source :
ChemInform. 30
Publication Year :
2010
Publisher :
Wiley, 2010.

Abstract

Glyoxylates of three chiral alcohols were conveniently prepared by reaction of the alcohol with oxalyl chloride followed by reduction of the resulting alkoxy oxalyl chloride with tributyl- tin hydride. The products were isolated in 75-80% yield by straightforward flash chromatography.

Details

ISSN :
15222667 and 09317597
Volume :
30
Database :
OpenAIRE
Journal :
ChemInform
Accession number :
edsair.doi...........98e7d852e7f1419b0d5ef9bd2c5e0536
Full Text :
https://doi.org/10.1002/chin.199909087