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Simple synthesis of quinolines and dibenzo[b,f][1,5]diazocines under microwave irradiation

Authors :
Yun-Young Kim
Yong-Gyun Lee
Dai-Il Jung
Jung-Tai Hahn
Do-Hun Lee
Eon-Jin Lee
Ju-Hyun Song
Source :
Tetrahedron Letters. 50:5805-5807
Publication Year :
2009
Publisher :
Elsevier BV, 2009.

Abstract

Quinolines 3a–f, 5a–f, and dibenzo[b,f][1,5]diazocines 4, 6 were synthesized in the presence of 0.5 equiv. of diphenyl phosphate (DPP) under microwave irradiation. The obtained yield of 6,12-diphenyl-dibenzo[b,f][1,5]diazocine 4 was higher when using anhydrous DPP than when using HCl, H3PO4, and CH3COOH.

Details

ISSN :
00404039
Volume :
50
Database :
OpenAIRE
Journal :
Tetrahedron Letters
Accession number :
edsair.doi...........b46b16d1b33a689ceaba72280890d859
Full Text :
https://doi.org/10.1016/j.tetlet.2009.07.150