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The Structure and Tribological Properties of Ni/MoS2 Composite Layers Formed on Aluminum and Its Alloys

The Structure and Tribological Properties of Ni/MoS2 Composite Layers Formed on Aluminum and Its Alloys

Authors :
M. Szumiata
B. Kucharska
J. R. Sobiecki
A. Zagórski
J. Mizera
Source :
Lecture Notes in Mechanical Engineering ISBN: 9789811361326
Publication Year :
2019
Publisher :
Springer Nature Singapore, 2019.

Abstract

This work investigates the influence of process parameters on microstructure, adhesion of layers to the substrate and wear resistance of Ni/MoS2 micro- and nanocrystalline composite layers. Pure nickel coatings were also fabricated and tested for comparison. The layers were deposited by electrochemical reduction on pure A2 aluminum and on PA6 alloy. The layers were produced at a current density of 3 A/dm2 and a mixing speed of 400 rpm. The bath composition was also modified by the addition of saccharin and the disperse phase of molybdenum disulfide in the bath (2.5 and 5 g/l). Materials prepared in this way underwent structural investigations (using scanning electron microscopy and optical microscopy), a scratch test and tribological tests (using a ball-on-disc method). The results of the tests allowed to determine the dependence of the structure and properties of the produced coatings on the production parameters. The composition of the electrolyte affects the size of crystallites as well as the morphology and topography of the surface. The scratch test confirmed the good adhesion of the nickel and composite layers to the substrate. The best lubricating properties were shown by nanocrystalline coatings. The too high content of molybdenum disulfide in the bath caused an undesirable increase in the coefficient of friction.

Details

Database :
OpenAIRE
Journal :
Lecture Notes in Mechanical Engineering ISBN: 9789811361326
Accession number :
edsair.doi...........c51c32f1a11e153d2ad33a8ed0f2a3cb
Full Text :
https://doi.org/10.1007/978-981-13-6133-3_14