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Dialkylamido Sulfoxylic Acid Fluorides, I: Synthesis and Reactions with Olefins

Authors :
Alexander B. Rozhenko
Yuriy G. Shermolovich
Vladimir N. Kozel
Valerij E. Pashinnik
Source :
Phosphorus, Sulfur, and Silicon and the Related Elements. 184:1149-1160
Publication Year :
2009
Publisher :
Informa UK Limited, 2009.

Abstract

The reaction of potassium fluoride with the corresponding acid chlorides results in the formation of dialkylamido sulfoxylic acid fluorides Alk 2 N-S-F. Stereo- and regioselectivity of dimethylamido and diisopropylamido sulfoxylic acid fluorides addition reactions to the C,C double bond in cyclohexene, 3,4-dihydro-2H-pyrane, and vinyl ethyl ether has been investigated. This reaction is a convenient approach to the β -fluoroalkyl sulfenic acid derivatives.

Details

ISSN :
15635325 and 10426507
Volume :
184
Database :
OpenAIRE
Journal :
Phosphorus, Sulfur, and Silicon and the Related Elements
Accession number :
edsair.doi...........db9a33e40a8de1bdecd4767d638c81cd
Full Text :
https://doi.org/10.1080/10426500902855182